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X-ray powder diffraction analysis of a nonlinear optical material 3-nitro–4-hydroxy–4′-bromobenzophenone

Published online by Cambridge University Press:  10 January 2013

Zong-ming Jin ,
Zheng Jin  and
Xiang-yin Zhou
Zong-ming Jin
Affiliation:
Central Laboratory, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
Zheng Jin
Affiliation:
Suzhou Testing Institute of Technology, 5 Minzhi Road, Suzhou, 215006, People's Republic of China
Xiang-yin Zhou
Affiliation:
Department of Chemistry, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
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Abstract

A nonlinear optical material 3-nitro–4-hydroxy–4′-bromobenzophenone has been characterized by x-ray powder diffraction. Experimental values of 2θ, corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 109 observed reflection with 2θ up to 90° are reported. The powder diffraction data have been evaluated, and the figures-of-merit are reported. The unit cell parameters least-squares refined from 34 nonoverlapping peaks of the orthorhombic compound with a P212121 space group are a = 7.619(7) Å, b = 27.651(5) Å, c = 5.650(7) Å, V = 1190.5(9) Å3, Z = 4, and Dx = 1.389 g/cm3.

Type
Research Article
Information
Powder Diffraction , Volume 10 , Issue 2 , June 1995 , pp. 117 - 119
Copyright
Copyright © Cambridge University Press 1995

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References

Appleman, D. E., and Evans, H. T. Jr., (1973). “Indexing and Least-Squares Refinement of Powder Diffraction Data,” Rep. PB 216188, U.S. Department of Commerce, National Technical Information Service, 5286 Port Royal Rd., Springfield, VA 22151.Google Scholar
de Wolff, P. M. (1968). “A Simplified Criterion for the Reliability of a Powder Pattern Indexing,” J. Appl. Cryst. 1, 108.CrossRefGoogle Scholar
Fei, Y. W., Yang, F., and Yu, C. X. (1989). “Organic and Polymeric Laser Materials for SHG,” Materials Sci. Progr. (in Chinese) 3, 255.Google Scholar
Smith, G. S., and Snyder, R. L. (1979). “FN: A Criterion for Rating Powder Diffraction Patterns and Evaluating the Reliability of Powder Pattern Indexing,” J. Appl. Cryst. 12, 60.CrossRefGoogle Scholar
Werner, P. F. (1984). “TREOR, Trial and Error Program for Indexing of Unknown Powder Patterns,” University of Stockholm, S 106 91, Stockholm, Sweden.Google Scholar