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X-Ray Powder Diffraction Data for (1R,2R) -(−)-norpseudoephedrine hydrochloride, (lS,2R)-(+)-norephedrine hydrochloride, and (±)-norephedrine hydrochloride

Published online by Cambridge University Press:  10 January 2013

D.F. Rendle ,
E.J. Glazier  and
P.M. Cain
D.F. Rendle
Affiliation:
The Metropolitan Police Forensic Science Laboratory, 109, Lambeth Road, London SEl 7LP, U.K.
E.J. Glazier
Affiliation:
The Metropolitan Police Forensic Science Laboratory, 109, Lambeth Road, London SEl 7LP, U.K.
P.M. Cain
Affiliation:
The Metropolitan Police Forensic Science Laboratory, 109, Lambeth Road, London SEl 7LP, U.K.
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Abstract

X-ray powder diffraction data for the three title compounds are reported. The crystals of all three compounds are monoclinic and the space group is P21 (No. 4) in each case. (1R, 2R)-(−)- norpseudoephedrine hydrochloride has a = 5.4422(8) Å, b = 8.071(1) Å, c = 11.839(1) Å and P= 101.803(9)°. For (1S,2R)-(+)-nqrephedrine hydrochloride a = 8.457(1) Å, b = 10.337(2) Å, c = 12.575(3) Å, and β = 107.46(1)° and for(±)-norephedrine hydrochloride a = 7.4406(6) Å, b = 9.4557(6) Å, c = 14.5799(8) Å and β= 103.446(7)°.

Type
Research Article
Information
Powder Diffraction , Volume 7 , Issue 1 , March 1992 , pp. 28 - 31
Copyright
Copyright © Cambridge University Press 1992

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References

Appleman, D.E. & Evans, H.T. (1973). NTIS Documen t No. PB-216118.Google Scholar
Benoit, P.H. (1987). Am. Mineral. 72, 1018–19.Google Scholar
Herbert, H. (1979). Acta Crystallogr. B35, 2054–2058.CrossRefGoogle Scholar
Folen, V. (1975). J. Forensic Sci. 20, 348–372.CrossRefGoogle Scholar
McMurdie, H.F., Morris, M.C., Evans, E.H., Paretzkin, B. & Wong-Ng, W. (1986). Pow. Diff. 1, 40–43.CrossRefGoogle Scholar
Smith, G.S. & Snyder, R.L. (1979). J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar
Welton, J. & McCarthy, G.J. (1989). Powder Diffraction File, No. 39-1504.Google Scholar